Instrumental Analysis
CHEM 336

• Syllabus 2007 Syllabus for the course
• Oral Final Exam  Web page containing the Final Exam Questions - Not used S-2007
• Textbook:  Quantitative Chemical Analysis; D. Harris
                      Electronic Text: Word files
                          Chapter 1:  Introduction
                          Chapter 2:  Measurements
                          Chapter 3:  Electronics Fundamentals
                          Chapter 4:  Computer Interfacing
• Optional Textbook: pdf files
                          DC Fundamentals
                          AC Fundamentals
                          Semiconductors and Operational Amplifiers
                          Digital Fundamentals
                          References

• Quiz Answers
      Quiz 1, answer in text
      Quiz 2
      Quiz 3
      Quiz 4
      Quiz 5

• Lab Handouts

Electronics 1 - Simple Spectrometer

Applied Electronics: Construction of a Simple Spectrophotometer; Melissa A. Thal, Michael J. Samide; J. Chem Ed. Vol 78, No 11, November 2001
591 LED
HLMP 3316
TLV 5300
VT 935G
HLMP 3750-3790
LM 741 Operational Amplifier
Allied Electronics Catalog Pages, LED1, LED2, Transducers, Power Supply
PhotoDiode Characteristics
Common Resistor Values

Spectrophotometric

Spectrophotometric Determination of the Dissociation Constant of an Acid–Base Indicator Using a Mathematical Deconvolution Technique, Krystyn P. Alter, John L. Molloy, and Emily D. Niemeyer*; J Chem Ed, Vol 82, No 11, November, 2005, p1682
 

HPLC

J Chem Ed, Vol 75, No 4, April 1998
J Chem Ed, Vol 60, No 2, February 1983

Atomic Absorption

Atomic Absorption Introduction - Introductory Lab - Read before coming to Lab
Manual for SpectrA-220
 

Electrochemical

Introduction to Electrochemistry- Read before coming to Lab
Introductory Lab for Cyclic Voltammetry- Read before coming to Lab

GCMS

Use of Solid-Phase Microextraction for the Quantitative Determination of Herbicides in Soil and Water Samples; Felix Hernandez,* Joaquim Beltran, Francisco J. Lopez, and Jose V. Gaspar, Anal. Chem, Vol 72, 2000

Solid-phase microextraction and gas chromatography with mass spectrometric detection for the determination of pesticides in aqueous samples; C. Aguilar*, S. Pen˜alver, E. Pocurull, F. Borrull, R.M. Marce; J Chrom A, vol 795, 1998

• Electronics Readings

                Common Resistor Values
                Cover - Credits for Information
                DC Circuits
                AC Circuits
                Operational Amplifiers
                Diodes
                     Problem Set 1 Answers Corrected 2/4/04
                     Problem Set 2 Answers

• Powerpoint Presentations
          Analog Electronics 
          Digital Electronics
          Potentiometry
          Potentiometry Problems
          Electrolysis
          Voltammetry
          Introduction to Spectroscopy
          Basic Construction of Spectrometer
          Atomic Spectroscopy
          Molecular Spectroscopy  
          Mass Spectrometry
          Separation Fundamentals 
          Gas Chromatography  - Problem Answers
          HPLC
          Setting Up Method
          Capillary Electrophoresis   
         
         
• J. Chem. Ed On-line access to J. of Chemical Education - Name:MICHAEL R ROSS
                                                                                                  Password: 26533
• Instrument Components Inside look at several instruments
• Library Holdings of Books dealing with Instrumental Analysis
• LCGC North America: Magazine that reviews current areas of interest in LC and GC